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Manual |
X-RaY crystallography FACILITY, Kasha Laboratory
Institute of Molecular Biophysics
Data Collection & Processing Guide
Macromolecular x-Ray Facility Crystallography Facility
Data Collection & Processing Guide
Copyright ã 2000-2004 Thayumanasamy Somasundaram
410-414 Kasha Laboratory • Institute of Molecular Biophysics
E-mail: soma@sb.fsu.edu
• URL: http://www.sb.fsu.edu/~soma
Phone 850.644.6448 • Fax 850.644.7244
September 28, 2004
Table of Contents
Introduction i
Purchase Orders & Blanket Orders
3. Regular data collection procedure
IP (Windows
NT, anaconda.chem.fsu.edu)
CCD (Linux,
spruce.chem.fsu.edu)
4. High-& Low-resolution data collection procedures
5. Low (cryo) temperature data collection procedure
Writing a
tape using DDS3 tape drive (raccoon.chem.fsu.edu)
Extracting
(reading) from tape
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Chapter 1 |
Facility Information & Contact Numbers
This chapter deals
with the Information about the X-Ray Crystallography Facility and the names and
contact numbers of relevant people.
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t |
he
X- Ray Facility (XRF) established in
1993 is located on the fourth floor of, Kasha Laboratory, Institute of
Molecular Biophysics. It occupies ~1200 ft2
of space spread among four different rooms KLB 410, 411, 412, & 413. It is a multi user macro-molecular x-ray
diffraction laboratory equipped with three copper rotating anode generators
(Rigaku H2Rs and Elliott GX-20), one R-Axis IIc image plate (IP) detector and one Mar165 charge-coupled device (CCD) detector. The x-ray generators
are coupled to either Osmic Confocal
The
facility provides the following services:
1. Single crystal (capillary or loop mounted) x-ray diffraction data collection